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Aurora 1030W TOC Analyzer

 

Aurora 1030W TOC Analyzer

 

The Aurora 1030W Total Organic Carbon (TOC) Analyzer uses the proven heated persulfate wet oxidation technique to analyze organic contamination levels in aqueous samples.

 

Virtually all organic compounds dissolved in water can be oxidized by heated sodium persulfate (Na2S208). Concentrated solutions (1 or 1.5 M) can effectively oxidize organic matter present in the form of colloids, macromolecules, and suspended solids.

 

The Aurora 1030W can be programmed and calibrated to analyze samples containing organic carbon at levels as low as 10 ppb and up to 30,000 ppm. Depending upon method and application, up to 300 samples can be analyzed in a 24-hour period.


The reaction chamber of the Aurora 1030W is thoroughly rinsed between analyses to eliminate residue from the previous sample. This ensures the Aurora 1030W maintains the low system background necessary for high sensitivity TOC measurements. This contrasts with combustion TOC analyzers in which residual salts accumulate on catalyst surfaces, degrading oxidation efficiency and causing higher blanks and background contamination.

 

Test Methods Supported by the Aurora 1030W TOC Analyzer

The heated persulfate oxidation technique has been approved and adopted in numerous regulatory compliance methods, standards, and norms for water quality testing.

 

Standard Method 5310C

Drinking Water / Wastewater

USEPA 415.3

Drinking Water

USP <643> / EU 2.2.44

Purified Water

ASTM D 4779

Ultrapure Water

ASTM D 4839

Wastewater, Seawater

USEPA-DBPR

Disinfection Byproduct Rule

USEPA-SPCC

Spill Prevention & Control Countermeasures

ISO 8245

Drinking Water, Wastewater

EN 1484

Surface & Ground Waters, Potable Water

 

The Aurora 1030W can be equipped with a number of instrument options and automation accessories to improve sample throughput and productivity.
· An optional second oxidation chamber supports concurrent sample processing.
· An 88-position rotary autosampler fits directly underneath the 1030W to conserve bench space.
· ATOC software provides 21 CFR Part 11 compliant data handling, security, auditing, and reporting capability.
· An optional validation package provides complete IQ / OQ / PQ documentation to validate an Aurora 1030W for use in pharmaceutical GLP/GMP applications.
· Multi-stream sampling module for at-line monitoring of up to four process streams.
· 1030S Solids Module operates in conjunction with a 1030W analyzer to combust solid materials for analysis of TC or TOC.
· Accessory kits to configure and interface a 1030W to an Isotope Ratio Mass Spectrometer (IRMS) or Cavity Ring Down Spectrometer to measure TOC and the δ13C stable isotope ratio.

 

Aurora 1030W Specifications

 

Operating Principle

 Heated sodium persulfate oxidation

 Measurement Technique

 Non-dispersive infrared (NDIR) detection

 Measurement Range

 10 ppb C – 30,000 ppm C (multiple calibration ranges or dilution required)

 Instrument Detection Limit (IDL)

 2 ppb C

 Operator Interface

 Color LCD touchscreen display with Windows® CE-based software

 Operating Modes

 Standalone (Windows® CE), PC-controlled, or LAN/LIMS network connectivity

 Basic Software

 Single instrument operation with data transfer to PC

 Optional ATOC Software

 Network LAN/LIMS operation, data management, custom reports, and 21CFR11 compliance

 Autosampler

 88 position rotary autosampler designed to fit directly underneath Aurora 1030W analyzer

 Sample Injection

 Manual syringe, sipper tube, autosampler, or multi-stream at-line sampling module

 Certification

 CE, EMC: EN61326 / Safety: IEC 61010-11 2001

 Reagents Required

 Sodium persulfate, 5% phosphoric acid, rinsewater

 Sample Injection Volume

 10μL – 10mL

 Method TC

 Acid and persulfate reaction

 Method TIC

 Acidification with Phosphoric acid and sparging

 Method TOC

 NPOC by heated persulfate oxidation or TC-TIC

 Heating

 Adjustable to 100 ˚C in 1˚C increments

 Repeatability

 2.0% or 2 ppb, whichever is greater

 Linearity

 ±1% FS or 2% relative, whichever is greater

 Sample pathway

 Color coded Teflon® tubing

 Sample handling

 Syringe with isolation loop to prevent contamination

 Gas Supply

 N2 (99.998%), zero-grade air, or O2 (99.998%)

 Power Supply

 Variable voltage, 100-240VAC, 50/60 Hz, 950W

 Dimensions – Aurora 1030

 42.5 cm H x 49.5 cm W x 41.9 cm D(16.75 in. H x 19.5 in. W x 16.5 in. D)

 Dimensions – Aurora 1030 + 1088 Autosampler

 26.75 in. H x 19.5 in. W x 23 in. D

 Weight – Aurora 1030 + 1088 Autosampler

 15.4 kg (34 lbs.), 34.5 kg (76 lbs.) 1030W + 1088

 

Methode Sample / Application
 Standard Method 5310C   Drinking Water / Wastewater 
 USEPA 415.3   

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Aurora 1030C (TNb) Module
1030S Solids Analysis Module
Model 1096+ XYZ TOC Autosampler
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